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Tributyl(Methyl)Ammonium Dicyanamide

    • Product Name Tributyl(Methyl)Ammonium Dicyanamide
    • Alias Cyrene Amberlyst
    • Einecs 629-426-0
    • Mininmum Order 1 g
    • Factory Site Tengfei Creation Center,55 Jiangjun Avenue, Jiangning District,Nanjing
    • Price Inquiry admin@sinochem-nanjing.com
    • Manufacturer Sinochem Nanjing Corporation
    • CONTACT NOW
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    Specifications

    HS Code

    162602

    Product Name Tributyl(Methyl)Ammonium Dicyanamide
    Cas Number 58261-74-6
    Molecular Formula C16H33N5
    Molar Mass 295.47 g/mol
    Appearance Colorless to pale yellow liquid
    Density 0.96 g/cm3 (approximate)
    Melting Point -30°C (approximate)
    Boiling Point Decomposes before boiling
    Solubility In Water Miscible
    Refractive Index 1.441 (approximate)
    Chemical Classification Ionic liquid
    Synonyms TBMA Dicyanamide

    As an accredited Tributyl(Methyl)Ammonium Dicyanamide factory, we enforce strict quality protocols—every batch undergoes rigorous testing to ensure consistent efficacy and safety standards.

    Packing & Storage
    Packing 250g of Tributyl(Methyl)Ammonium Dicyanamide supplied in a tightly sealed amber glass bottle with clear hazard labeling and safety instructions.
    Shipping Tributyl(Methyl)Ammonium Dicyanamide should be shipped in tightly sealed containers, protected from moisture and incompatible substances. Handle as a chemical substance requiring standard precautionary measures. Transport according to local, national, and international regulations, such as DOT, IATA, or IMDG, typically as non-hazardous, but confirm with the Safety Data Sheet (SDS) for specifics.
    Storage Tributyl(Methyl)Ammonium Dicyanamide should be stored in a cool, dry, and well-ventilated area, away from direct sunlight and sources of ignition. Keep the container tightly closed and properly labeled. Avoid contact with strong oxidizing agents and moisture. Use suitable, chemical-resistant containers to prevent leakage or degradation. Store according to local regulations and manufacturer's guidelines for safe chemical handling.
    Application of Tributyl(Methyl)Ammonium Dicyanamide

    Applications of Tributyl(Methyl)Ammonium Dicyanamide in Industrial Manufacturing

    Tributyl(Methyl)Ammonium Dicyanamide has proven utility in several specialized chemical industries as a phase transfer catalyst and ionic liquid precursor, valued for enabling efficient processing in diverse formulations. Below we detail real-world application scenarios, providing technical insights on required industry standards, recommended incorporation levels, downstream processing steps, and resulting end products.

    1. Electrolyte Component in High-Performance Lithium-Ion Batteries

    This raw material finds demand as an additive and precursor in advanced non-aqueous electrolyte formulations for lithium-ion batteries, supporting ion conductivity and thermal stability. Battery manufacturers source it to fine-tune cycling performance and improve safety margins, particularly in high-energy-density cell designs for automotive and energy storage applications.

    Industry compliance standards

    • IEC 62660: Secondary Lithium-ion cells for the propulsion of electric road vehicles
    • UN 38.3: Recommendations on the Transport of Dangerous Goods Manual of Tests and Criteria
    • RoHS (Restriction of Hazardous Substances Directive, 2011/65/EU)
    • Relevant REACH registrations for chemical safety

    Typical usage ratio

    • 0.1–1.5% by weight in the total electrolyte solution, subject to target conductivity and electrochemical performance; formulators adjust concentration based on desired SEI (solid-electrolyte interphase) modification and stability requirements.

    Downstream process integration

    • Add to the electrolyte mixing tank after solvent blending and lithium salt dosing; operators control temperature and mixing speed to ensure complete dissolution before final quality analysis and electrolyte filling into cell assemblies.

    Final product types

    • Prismatic lithium-ion battery cells for electric vehicles
    • Cylindrical lithium-ion cells for power tools
    • Pouch-type lithium-ion cells for stationary storage systems
    • High-rate batteries for consumer electronics

    2. Ionic Liquid Precursor for Metal Catalysis and Surface Treatment

    The material acts as a synthetic intermediate in custom ionic liquid formulations, which downstream producers use for metal catalyst systems in industrial surface finishing and plating baths. Its integration allows for enhanced ionic conductivity and facilitates catalytic cycles that improve plating uniformity and reduce processing defects in microelectronics and aerospace component manufacturing.

    Industry compliance standards

    • ISO 6158: Electroplated coatings of nickel and nickel alloys
    • ASTM B488: Electrodeposited coatings of gold for engineering uses
    • Directive 2011/65/EU (RoHS) for heavy metal content in electronics
    • Process-specific OEM specifications in electronics manufacturing

    Typical usage ratio

    • 5–25 mol% as an ionic liquid cation source in custom catalyst or plating bath preparations, dependent on specific plating metal and current density requirements.

    Downstream process integration

    • Producers synthesize custom ionic liquids by reacting dicyanamide salt with various counterions before introducing the blend to the catalyst system or plating tank; the compound is typically diluted with appropriate solvent and complexed with target metal ions in controlled temperature environments.

    Final product types

    • Microelectronic circuit boards with fine metal features
    • Aerospace-grade plated fasteners and connectors
    • Automotive sensor components with specialty coatings
    • Gold-plated connector pins for data transmission interfaces

    3. Reaction Medium in Pharmaceutical Fine Chemical Synthesis

    Tributyl(Methyl)Ammonium Dicyanamide is specified as a non-protic, high polarity organic phase transfer agent for certain active pharmaceutical ingredient (API) syntheses, where it can reduce by-product formation and increase yields in nucleophilic substitution and cyclization reactions. Pharmaceutical API producers employ it in process steps that require strict control over impurity levels and solvent residues.

    Industry compliance standards

    • ICH Q7: Good Manufacturing Practice for Active Pharmaceutical Ingredients
    • European Pharmacopoeia (Ph. Eur.) solvent residue limits
    • US FDA cGMP (21 CFR Parts 210 & 211)
    • ISO 9001: Quality Management in the pharmaceutical supply chain

    Typical usage ratio

    • 0.5–8% w/w in reaction mixtures, subject to stoichiometry and lab scale-up validation during process verification; actual usage tailored to the reactivity of nucleophilic intermediates.

    Downstream process integration

    • Operators introduce the phase transfer agent to the reaction vessel after charging reactants and base, optimizing stir rate and temperature profiles; post-reaction, the batch undergoes work-up to separate product and purify the API in compliance with GMP requirements.

    Final product types

    • Antiviral small molecule intermediates
    • Pyrimidine- and triazine-based pharmaceutical actives
    • Specialty fine chemicals for downstream formulation
    • Chiral building blocks for peptide therapeutics

    4. Additive in High-Performance Polymer Manufacturing

    Chemical processors utilize Tributyl(Methyl)Ammonium Dicyanamide during the synthesis of high-performance polymers and specialty resins, leveraging its phase transfer and ionic modification capabilities to control molecular weight and dispersion properties. This application is increasingly relevant in the manufacturing of engineering plastics destined for automotive, electronics, and aerospace markets where consistency and batch traceability are critical.

    Industry compliance standards

    • ISO 9001 and ISO 14001 for quality and environmental management in polymer production
    • UL 94: Flammability standards for plastics materials
    • REACH Annex XVII for chemical content restrictions
    • OEM requirements for automotive and E&E components

    Typical usage ratio

    • 0.05–0.8% by weight, custom-tuned depending on target polymer backbone and desired melt flow index; higher concentrations typically reserved for specialty high dielectric or antistatic grades.

    Downstream process integration

    • Dosed into the monomer mix during the in-situ polymerization stage, prior to chain initation; quality control labs monitor viscosity and compositional uniformity before molding or extrusion into finished parts.

    Final product types

    • Engineering polyimide and epoxy resins for circuit substrates
    • High-durability automotive under-hood plastics
    • Electronic housings requiring antistatic performance
    • High-performance coatings for industrial rollers

    5. Phase Transfer Catalyst in Agrochemical Intermediate Production

    Manufacturers in the agrochemical sector employ this raw material to optimize the yield and purity of key pesticide and herbicide intermediates, particularly for reactions involving non-polar reactants or where water-organic phase separation limits classical pathways. The compound improves process economics by enabling lower reaction temperatures and reducing batch times.

    Industry compliance standards

    • FAO/WHO pesticide specifications
    • ISO 9001: Quality Management for crop protection products
    • REACH authorization for all precursor chemicals
    • Process Hazard Analysis (PHA) as per OSHA 1910.119

    Typical usage ratio

    • 0.3–2.0% of total batch mass, adjusted according to reaction kinetics, target yields, and downstream purity requirements in intermediate synthesis.

    Downstream process integration

    • Added after main reactant charging; batch reactors fitted with vigorous agitation ensure miscibility, and downstream separation units recover final product and residual catalyst for waste minimization and compliance reporting.

    Final product types

    • Selective herbicide intermediates for cereal crops
    • Insecticide precursors for soil treatment
    • Fungicide building blocks for post-harvest treatment

    6. Accelerator in Photopolymer Resin Formulation for 3D Printing

    This substance is increasingly utilized as an ionic additive in the formulation of UV-curable photopolymer resins, improving cure rate, dimensional accuracy, and interlayer adhesion for additive manufacturing. Resin formulators apply it in precise concentrations to enhance feature resolution in microprinting and dental appliance production.

    Industry compliance standards

    • ISO/ASTM 52900: Additive manufacturing — General principles
    • ISO 10993 for biocompatibility of dental materials
    • Quality audits under ISO 13485 for medical device parts
    • RoHS for electrical and electronic component applications

    Typical usage ratio

    • 0.02–0.15% by total resin weight, established during pilot-scale validation to balance curing depth with print speed and mechanical testing outcomes.

    Downstream process integration

    • Typically incorporated during the resin pre-mix stage under UV-safe conditions; formulating engineers verify reactivity through real-time photorheometry tests prior to batch-scale production.

    Final product types

    • High-resolution 3D-printed dental aligners and crowns
    • Precision micro-mechanical parts for electronics
    • Functional prototype components for automotive R&D
    • Custom-fit hearing aid shells and medical guides
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    Certification & Compliance
    More Introduction

    Tributyl(Methyl)Ammonium Dicyanamide: Building Chemical Solutions from Experience

    As chemical manufacturers, we measure our success by the solutions we create and the consistency we deliver. Tributyl(methyl)ammonium dicyanamide stands out in our lineup not just for what it does, but for how it gets the job done right in demanding industrial and laboratory environments. The chemical isn’t just an entry in a catalog—it represents real hours spent scaling reactions, monitoring purity, and tweaking yields within the walls of our own plants.

    Inside Our Manufacturing Floor

    We run hundreds of controlled syntheses every year. Tributyl(methyl)ammonium dicyanamide comes to life here, not as a curiosity, but as a tool shaped by specific needs. Over many batches, we’ve controlled the hydrolysis step to keep water content within specs; we’ve sharpened purification cycles to strip off byproducts; we’ve documented color, odor, and solubility to make sure each drum matches the next. This hands-on experience gives us the confidence to share not just a chemical, but a process that works reliably in the field.

    Molecular Details, Practical Impact

    Its formula—C14H29N5—gains significance only through function. We measure its melting point, check dicyanamide content, and monitor whether the solution remains clear after weeks in storage. Each check matters since a deviation means wasted time—and those delays ripple out beyond our doors. Our own reports on batch consistency help customers avoid unnecessary retesting, especially in sensitive applications like ionic liquids, custom electrolytes, or organometallic synthesis.

    What Our Customers Tell Us—and What We Learn

    Customers have used tributyl(methyl)ammonium dicyanamide in processes demanding more than a simple ionic liquid. The dicyanamide anion brings special attributes to the table—not all ammonium salts will work in high-conductivity conditions. Technicians running pilot lines have noticed improved solubility for niche catalysts; research labs come back for its stability in high-voltage electrolytes. These reports guide our quality focus. When someone runs a run that fails, we hear about it. We set up our own internal trials, pushing the chemical’s limits with thermal cycling, exposure to trace acid, or aging tests to be sure the product in our customer’s hands performs to the same standard as the one sitting with our chemists.

    Not Just Another Ammonium Salt

    Comparing this product to industry basics helps illustrate its value. For example, standard tetraalkylammonium salts, such as tetrabutylammonium bromide, just don’t offer what the dicyanamide group supplies. Our customers in advanced materials synthesis stress over the wrong anion stalling their reactions or corroding specialized equipment. Simpler salts might dissolve quickly, but lack the unique charge-transfer properties or low viscosity needed for custom catalytic or electrochemical projects. We’ve worked with process chemists who swapped from bromides or perchlorates to tributyl(methyl)ammonium dicyanamide, simply because they reached temperature or solubility thresholds the old salts couldn’t meet.

    On the cation side, the presence of a methyl group alongside three butyls isn’t arbitrary—it hinges on trial and error with side-chain length and charge density. Longer chains usually push the melting point lower, but sometimes at the expense of solubility or phase stability. The methyl branch lets customers balance cost, handling, and reactivity without growing impurities or build-up in their systems. We’ve run side-by-side batch syntheses in house: the methyl variant flows more easily than the straight tetrabutyl counterparts, grants better cold-flow properties, and—according to a customer in battery research—allows their system to run between cycles without salt precipitation. These are details learned on the job, not in textbooks.

    Direct Experience with Usage in the Field

    Electrolyte developers make up a growing share of our customer base. Battery R&D teams push us for high purity and tight control of dicyanamide content, since even trace acids destabilize cycling. Advances in supercapacitors and flow batteries ride on optimizing anions for voltage stability; after a customer’s heartfelt troubleshooting session or two, we adjusted our process to cut moisture even further, delivering drums sealed under nitrogen instead of ambient air. Our warehouse now carries a dedicated cabinet for sensitive ammonium salts, and our crew tracks shelf life and exposure—those are details that affect how well the chemical works inside a battery test cell, not just on a certificate of analysis.

    Beyond energy storage, fine chemical synthesis teams leverage tributyl(methyl)ammonium dicyanamide as a phase-transfer catalyst or as a base in specialist couplings. Their operations hinge on avoiding trace chlorides or sodium ions, which we discovered the hard way during scale-up trials in our own lab. A small tweak in the filtration protocol allowed us to offer a low-sodium version. That not only unlocked a new market, but cut down on customer complaints when sensitive reactions started behaving strangely. Over time, customer feedback led us to keep three grades on hand: technical, low-sodium, and low-moisture.

    Some users come to us from the world of polymer chemistry, where dicyanamide-based agents push forward crosslinking techniques under mild conditions. Their priorities differ: cost, viscosity at working temperature, and ease of mixing. We care not just about spec sheets but about how product flows through a pump or blends in a jacketed reactor. After a few rounds of customer meetings, we built up a technical library describing the real-world handling and blending quirks—not just abstract numbers but pressure drops, agitation rates, and observations on visual stability.

    Quality: Standards from Our Own Operations

    As manufacturers, we maintain stricter standards than a typical distributor. Each batch receives its own traceability tag, allowing us to follow the journey from raw material intake through synthesis, washing, and drying, all the way to packaging. We recognize trends in spectral data—minor shifts in IR or NMR signals alert us to impurities that could trip up sensitive downstream chemistry. Since the shelf life of dicyanamide-based salts depends on water ingress and light exposure, we’ve set up a facility protocol involving UV-shielding, controlled climate storage, and fast-turnover packaging. We only ship what has passed our internal benchmarks for purity and performance in application-specific tests, not just generic laboratory analysis.

    No process remains static. We adjust synthesis in response to both internal findings and customer pain points. If a research team finds their product yellowing over time, our technical team investigates sources of oxidative degradation, tweaks antioxidant additives, or revisits post-synthesis wash cycles. Opening the lines of communication with these partners leads to changes on our end—whether in reaction setup, filtration, or packaging. We document these changes, not just for legal compliance, but to improve the experience for those who rely on our product in high-value processes.

    Safety and Handling—Drawn from Shop Floor Lessons

    Every chemical comes with its real-world risks and challenges. On our shop floors, staff wear gloves and goggles not for show but because accidental dicyanamide skin contact brings a rash or irritation. We regularly re-evaluate material transfer protocols and spill response, since ammonium dicyanamide products left open to moist air clump fast and may hydrolyze. In our experience, minor spills clean up best with an inert absorbent, and it’s worth purging transfer lines with dry nitrogen before loading. These aren’t just bureaucratic rules—they came from workday realities, sometimes after a batch didn’t meet specifications or someone spent a shift hosing down sticky residue from a transfer vessel.

    Customers often ask about odor and environmental footprint. Tributyl(methyl)ammonium dicyanamide beats many alternatives on volatility and environmental discharge risk. Labs using chloride salts complain about persistent odors and stringent wastewater requirements—something we noticed in our pilot synthesis lines. By offering dicyanamide-based alternatives based on first-hand experience, we cut down on both plant odors and hazardous-waste disposal costs. This isn’t theoretical; our facility’s environmental audits improved year over year after the switch, helping both compliance and daily working conditions.

    Logistics and Storage—Practical Outcomes

    Manufacturing and supply-chain management operate hand-in-hand. Dicyanamide salts require careful packaging, especially during humid months. Early shipments taught us the hard way about condensation issues in tropical climates—those drums never reached their destination with the same free-flowing powder we packed. After a year adjusting shipment schedules and switching to foil-lined, double-sealed drums, we now ship product that holds up, whether it’s going to a city lab or a remote plant operating with intermittent power. Our warehouse teams check climate loggers on outgoing shipments, prevent extended warehouse holds, and track inbound humidity spikes. From these records, we learned to ship only full containers and avoid repacking until just before delivery.

    In-house storage solutions also matter. The staff in our own plants benefit from clear labeling, FIFO tracking, and using transfer lines with large, easy-flush bore. Product that cakes or clogs small hoppers causes downtime—these aren’t just theoretical inconveniences, but lost hours logged in maintenance calls and production delays. Because our team sees these troubles first-hand, we feed what we learn back into product support. Now, we supply users with storage guidelines based on actual outcomes, helping both small research labs and large production outfits avoid common pitfalls.

    Differences That Carry Weight in the Field

    Standing next to basic tetraalkylammonium salts, tributyl(methyl)ammonium dicyanamide follows a different script. Our R&D teams compared dissolution speeds in both organic and aqueous media for typical competitors; dicyanamide consistently cleared up faster, leaving less residue behind. Its electrochemical window covers a broader range, crucial for designers working on next-generation battery chemistries or advanced catalysis. Cost weighs in, too—our partners in scale-up operations care about the price per kilogram, but they also want less downtime spent troubleshooting solubility or stability failures.

    In years of direct manufacture and user feedback, certain differences keep coming up:

    Solutions Shaped by Manufacturer Experience

    Our approach grows not from generic guidance but from how we interact every day with the chemicals we produce. If a customer calls with a performance issue—reagent instability, solubility mismatch, or handling clog—the first reaction isn’t to drop a templated answer, but to review our production records, trial data, and hands-on troubleshooting notes. We’ve seen cases where warehouse temperature swings pushed the product out of spec; those prompted changes both in plant storage and suggested on-site protocols for our clients. Because we run these batches in our own facility, we continually adapt process steps, packaging solutions, and quality checks to fix real-world problems, not hypothetical flaws.

    Our technical team stands ready not with generic answers, but with a body of trial-and-error learning. For users working at the fringe—pushing solvent compatibility or testing edge-case reactions—we can describe what worked in our plants: which transfer solvents produced the cleanest recovery, what ambient conditions risked hydrolysis, and at what shelf life the product started drifting from the nominal grade. This depth of know-how only builds after years of direct engagement at the bench, in the warehouse, and alongside end users in the field.

    Summary: Why Tributyl(Methyl)Ammonium Dicyanamide Delivers

    Tributyl(methyl)ammonium dicyanamide doesn’t just slot into a generic ammonium salt application. It fills needs, supports discovery, and simplifies daily handling for those working on the cutting edge—chemists developing specialty electrolytes, engineers scaling up niche catalysts, or process operators mixing a slurry in a climate-challenged plant. Its value rests in more than molecular structure; it reflects lessons learned in real manufacturing settings: mistakes rectified, quality tightened, and feedback acted on.

    By making and using tributyl(methyl)ammonium dicyanamide in our own plant—and sharing practical know-how, not just paperwork—we offer not a commodity, but a solution shaped by the real demands of today’s chemical industry. Those in the field need more than just reliability; they need a partner who can troubleshoot, explain, and adapt, all the way from production line to application site. That’s what we strive to deliver, with tributyl(methyl)ammonium dicyanamide and every product that leaves our doors.