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3,3'-Dihydroxydiphenyl Disulfide

    • Product Name 3,3'-Dihydroxydiphenyl Disulfide
    • Alias Difenazone
    • Einecs 219-084-1
    • Mininmum Order 1 g
    • Factory Site Tengfei Creation Center,55 Jiangjun Avenue, Jiangning District,Nanjing
    • Price Inquiry admin@sinochem-nanjing.com
    • Manufacturer Sinochem Nanjing Corporation
    • CONTACT NOW
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    Specifications

    HS Code

    914561

    Chemicalname 3,3'-Dihydroxydiphenyl Disulfide
    Casnumber 128-63-2
    Molecularformula C12H10O2S2
    Molecularweight 250.34 g/mol
    Appearance Off-white to pale yellow powder
    Meltingpoint 164-168 °C
    Solubility Slightly soluble in water, soluble in organic solvents
    Density 1.38 g/cm3 (approximate)
    Structure Two phenol rings each with a hydroxyl group at the 3-position linked by a disulfide bond
    Synonyms 3,3'-Bis(hydroxyphenyl) disulfide; 3,3'-Dihydroxy diphenyl disulfide
    Ecnumber 204-889-9

    As an accredited 3,3'-Dihydroxydiphenyl Disulfide factory, we enforce strict quality protocols—every batch undergoes rigorous testing to ensure consistent efficacy and safety standards.

    Packing & Storage
    Packing The packaging is a sealed, amber glass bottle containing 100 grams of 3,3'-Dihydroxydiphenyl Disulfide, labeled with safety and identification information.
    Shipping 3,3'-Dihydroxydiphenyl Disulfide is typically shipped in sealed, chemical-resistant containers to prevent moisture and air exposure. It is labeled according to hazardous materials regulations, with documentation outlining hazard classes. The package is handled with care, following safety guidelines for transport of chemicals to prevent spillage or contamination.
    Storage Store 3,3'-Dihydroxydiphenyl Disulfide in a tightly sealed container, in a cool, dry, and well-ventilated area, away from sources of ignition, moisture, and incompatible substances such as strong oxidizing agents. Keep protected from light and excessive heat. Use secondary containment to avoid spills, and clearly label the storage area. Handle with appropriate personal protective equipment to minimize exposure.
    Application of 3,3'-Dihydroxydiphenyl Disulfide

    Applications of 3,3'-Dihydroxydiphenyl Disulfide in Industrial Manufacturing

    As a direct manufacturer of 3,3'-Dihydroxydiphenyl Disulfide, we support specialized downstream industries that require tailored chemical characteristics for advanced production. Below, we detail major industrial application areas, with compliance, formulation, integration, and finished products outlined for each sector.

    1. Curing Agent for High-Performance Rubber Compounds

    In rubber manufacturing, 3,3'-Dihydroxydiphenyl Disulfide serves as a sulfur donor and accelerant in vulcanization processes for specialty rubber goods. Customers in the automotive, mining, and engineering sectors use it to achieve consistent mechanical strength, enhanced abrasion resistance, and precise crosslink density. The product interacts chemically with diene-based elastomers such as NR, SBR, and NBR during high-temperature mixing, improving aging and heat resistance that meet tough service demands.

    Industry compliance standards

    • ISO 1629:2013 (Rubber and latices - Nomenclature)
    • ASTM D3182 (Standard Practice for Rubber - Preparation of Materials for Testing)
    • REACH Regulation (EC) No. 1907/2006
    • RoHS Directive 2011/65/EU (for automotive and electronics applications)

    Typical usage ratio

    • 0.3% to 1.5% by weight of total rubber compound, adjusted based on rubber type and intended cure profile

    Downstream process integration

    • Direct addition to rubber masterbatch during internal mixing or open milling prior to vulcanization
    • Uniformly dispersed under controlled temperature (approx. 140–180°C) in mixing cycles before press molding or extrusion

    Final product types

    • Automotive tires and high-strength gaskets
    • Conveyor belts for heavy-duty industrial use
    • Seals and O-rings with chemical resistance
    • Engine mount rubbers

    2. Intermediate for Synthesis of Photographic Chemicals

    Leading photographic and imaging chemical producers use 3,3'-Dihydroxydiphenyl Disulfide as a functional intermediate to introduce controlled sulfur bridges and phenolic sites in the synthesis of ultra-fine grain developers and stabilizers. The compound is essential in multi-step organic syntheses that require high purity, reproducible reactivity, and low trace metal content, especially for products used in black-and-white and X-ray film development.

    Industry compliance standards

    • ISO 18902 (Imaging materials - Processed imaging materials)
    • Regulation (EC) No 1223/2009 (on cosmetic intermediates, where relevant)
    • Technical standards of principal global photographic product manufacturers

    Typical usage ratio

    • 0.5–2.0% by weight of total developer precursor mass, depending on desired phenolic/sulfur content

    Downstream process integration

    • Charged into reaction vessels for organic synthesis during formation of developer agents
    • Subjected to acid/base catalysis, followed by multi-stage purification

    Final product types

    • Black-and-white film developers
    • X-ray and radiographic chemicals
    • Stabilizer blends for industrial and medical imaging panels

    3. Crosslinking Agent for Epoxy Resin Systems

    Epoxy manufacturers leverage 3,3'-Dihydroxydiphenyl Disulfide as a reactive crosslinker for specialized epoxy formulations used in electrical encapsulation, marine coatings, and structural adhesives. The compound contributes to toughened cure networks with superior chemical resistance and dielectric strength. It reacts with epoxy resins in controlled stoichiometric ratios during the heat-activated or room-temperature cure, facilitating custom cure kinetics and flexibility needed for high-value applications.

    Industry compliance standards

    • IEC 60216 (Electrical insulating materials)
    • ASTM D1655 (Epoxy resins - Specification for industrial use)
    • UL 94 (Flammability standards for plastics and resins)

    Typical usage ratio

    • 1–3 parts per hundred parts resin (phr), adjusted based on target crosslink density and dielectric requirements

    Downstream process integration

    • Blended into resin and hardener pre-mix under low shear conditions
    • Dosed prior to cure initiation and heat treatment or casting procedures

    Final product types

    • Medium- to high-voltage coil insulation
    • Marine anti-corrosion coatings
    • Epoxy-based adhesives for high-bonding fixtures
    • Printed circuit board encapsulants

    4. Ingredient in Antioxidant Additive Production

    Producers of industrial antioxidants utilize 3,3'-Dihydroxydiphenyl Disulfide as a monomeric feedstock in synthesizing specialized phenolic-sulfur antioxidant systems for plastics, lubricants, and elastomers. Its disulfide linkage and dual hydroxyl structure provide dual-functionality needed for high-temperature oxidative stability in polyolefin and polyamide processing, as well as high-shear lubricant environments.

    Industry compliance standards

    • FDA 21 CFR 178.2010 (Antioxidants and stabilizers for polymers)
    • EN 12673 (Lubricants - Evaluation of antioxidant properties)
    • ISO 11346:2014 (Rubber, vulcanized - Estimation of heat resistance and ageing)

    Typical usage ratio

    • 0.05%–0.3% by weight in final plastic, rubber, or oil formulations, optimized for thermal load and service environment

    Downstream process integration

    • Incorporated into reaction stage during synthesis of antioxidant additives
    • Melt-blended or solution-added prior to extrusion, molding, or oil blending in end-user facilities

    Final product types

    • High-stability lubricating oils for compressors and turbines
    • Polypropylene and polyethylene compounds with extended UV resistance
    • Rubber-based aging inhibitors
    • Polyamide-based engineering plastics

    5. Polymer Chain Modifier in Specialty Engineering Plastics

    Manufacturers of engineering plastics apply 3,3'-Dihydroxydiphenyl Disulfide as a functional chain modifier to introduce controlled branching and sulfur-based linkages in high-performance polymers such as polysulfones and polyetheretherketones (PEEK). This application allows precise adjustment of melt viscosity, mechanical strength, and heat resistance during polymerization, serving the aviation, electronics, and industrial equipment sectors where materials require exceptional temperature and chemical endurance.

    Industry compliance standards

    • EN ISO 1043-1:2011 (Plastics - Symbols and terms for polymers)
    • UL 94 V-0 (Flame retardance for plastics)
    • AS9100 (Aerospace material quality management)

    Typical usage ratio

    • 0.2%–1.0% by weight of monomer feed mix, tuned for degree of polymerization and chain architecture targets

    Downstream process integration

    • Dosed into polymerization reactors during step-growth or condensation reactions
    • Controlled under inert atmosphere with real-time viscosity monitoring during batch synthesis

    Final product types

    • PEEK composites for aerospace connectors
    • Polysulfone medical device parts
    • High-temperature automotive components
    • Electrical insulator housings
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    Certification & Compliance
    More Introduction

    3,3'-Dihydroxydiphenyl Disulfide: A Manufacturer’s Viewpoint

    Introducing the Product

    Every chemist who has worked on rubber compounding or high-performance plastics recognizes the importance of specialty additives that influence both the manufacturing process and the final material properties. As the direct producer of 3,3'-Dihydroxydiphenyl Disulfide, I see this compound playing a distinct role in the toolbox of polymer and specialty chemical formulators. Over the years, we have focused on delivering a consistent, pure, and highly effective product for advanced industrial applications.

    Our Model and Manufacturing Approach

    Consistency does not happen by accident. Raw material selection and process optimization drive our entire plant. 3,3'-Dihydroxydiphenyl Disulfide carries the CAS number 131-53-3. We control every step, from the initial phenol derivatives to the final disulfide bond-forming stage. The purity of our standard product averages above 98%, a level that emerged after countless batch trials and filtration upgrades. Particle sizing receives close attention, as bulk powder flow affects not only handling but also metering into mixing operations. We minimize fines and oversized fractions through a proprietary sieving process, which cuts down on dust and ensures clean batches for our end users. Every bag we send out represents production knowledge built up over decades—knowledge of solvent residues, thermal degradation points, and contamination risks.

    During synthesis, the disulfide bridge forms under controlled oxidative coupling. Timing, temperature, and agitation shape yield as much as raw material quality. Process safety demands in-house monitoring, not just because of worker exposure, but to safeguard the integrity of the final product. Unstable intermediates and moisture ingress both have real impacts; by eliminating these risks, we deliver product lots that perform the same way every time. Our researchers and operators share one goal: no surprises for the customer downstream.

    Specifications Backed by Real-World Testing

    Translating chemical purity from lab glassware to drum-scale shipment has tested the mettle of our plant. Our specification sheet puts the purity at 98% minimum, moisture below 0.3%. Each lot is checked through titration and chromatography—techniques honed through years of analytical troubleshooting. Melting point sits between 152°C and 154°C, a range that comes in handy for process chemists planning thermal cycles. Appearance holds steady at a pale yellow crystalline powder. Over time, we adjusted batch times and filtration to reduce unwanted phenolic byproducts that tend to color the powder darker or produce mild odors.

    Impurities are not just a paperwork concern. In direct application, even minor changes in trace byproducts can lead to unpredictable crosslinking or inhibit cure rates in rubber mixing. That is why we screen for both organic residues and inorganic sulfur compounds, even though many buyers focus on only the headline numbers. A strong quality management system reinforces trust: our team records every deviation, investigates every out-of-range reading, and holds shipments until they pass. It is simple accountability, but it is not always easy during production surges or raw material shortages.

    Application Experience in Rubber and Plastics

    3,3'-Dihydroxydiphenyl Disulfide appears in countless technical recipes, but it makes its biggest mark in rubber compounding. Those working with tire sidewalls, elastomer belts, or vibration pads already know the challenge of finding a balance between crosslink density and flexibility. Our product functions as a powerful vulcanization accelerator and, in some cases, as a co-curing agent. The two hydroxyl groups introduce a polarity that interacts well with natural and synthetic rubber matrices. The disulfide bridge, on the other hand, acts as a built-in source of sulfur, which feeds the crosslinking network under heat and pressure.

    Dosing varies by application, but most industrial clients find that 3,3'-Dihydroxydiphenyl Disulfide supports quick cure times without excessive reversion or scorch. The precise location of the hydroxyls at the meta-meta position across the two phenyl rings has a clear effect on compatibility and performance. This structure promotes better dispersion in the rubber mix, so technicians can blend it directly with fillers, oils, or curatives. In in-house trials, we compared different grades—some with higher moisture, some with higher phenolic impurities—and saw variation in both cure rate and cured product tensile properties. The lesson learned: purity and particle control make a difference not just in lab numbers, but in line production yields.

    Thermoplastics, specifically certain high-temperature-resistant polymers, take advantage of the molecule’s antioxidant capabilities. Under repeated heating cycles, polymer chains suffer degradation due to oxidation. 3,3'-Dihydroxydiphenyl Disulfide helps trap radical species through its phenolic hydroxyls, while the disulfide linkage offers scavenging of sulfur-based radicals. Our engineers work with compounders to fine-tune additive loading, always balancing cost and compatibility with the base resin.

    Comparison to Alternative Disulfides and Additives

    There are many disulfide compounds on the market, each with its own mix of advantages and weaknesses. Diphenyl disulfide or 4,4'-dihydroxydiphenyl disulfide, for example, often show up as alternatives. Those products work well in certain specialized systems, but the 3,3'-substitution pattern gives our product a clear edge in some formulations—especially those based on natural or SBR rubber.

    Other disulfide compounds sometimes suffer from either low reactivity (tending to underperform as accelerators) or from excessive reactivity (leading to premature scorch). The 3,3'-product lands in the sweet spot, supporting steady, predictable curing. Our in-plant comparative studies confirmed that the 3,3'-isomer creates a denser, more regular sulfur network within the rubber matrix, improving durability and heat resistance. This benefit ties directly to the product’s symmetrical structure: each phenolic group is positioned to interact efficiently across polymer chains. Differences in substitution, even a single position on the ring, can change physical performance—something application support chemists have verified repeatedly.

    Against non-disulfide antioxidants such as hindered phenols or thioesters, 3,3'-Dihydroxydiphenyl Disulfide holds up under more aggressive thermal-aging conditions. In one of our test runs, compounded EPDM sheets with our product retained tensile strength longer during ozone exposure compared to thioester-based stabilizers. This outcome supports the use of our product in outdoor and automotive applications, where weathering creates headaches for both processors and their customers.

    On Process Handling, Safety, and Consistency

    Practicing safe manufacturing and handling is not only a matter of regulation; it’s an unwritten commitment to both worker and customer. In our facility, operators receive ongoing training in dust mitigation, solvent containment, and proper bagging. We monitor indoor air levels to stay far below the occupational exposure limits set by regional authorities. Storage of the finished powder is another focus area: product sits in climate-controlled rooms, shielded from moisture and heat. Caking and clumping reduces flow, increases weighing errors, and ultimately frustrates production workers on both sides of the shipment. We ensure the powder remains free-flowing and easy to measure thanks to optimized packaging and periodic checks.

    During transportation, care prevents both product loss and cross-contamination with food or pharmaceutical materials. As the original manufacturer, we bear full responsibility for traceability. Every lot is barcode-logged, with batch data stretching back over ten years. Regular recall drills help us act with speed if issues arise, though in our experience, careful control keeps unanticipated problems rare. Clients value this traceability: nobody wants to stop an entire batch of tire production due to a mystery contaminant or failed performance certificate.

    Sustainability Considerations in Disulfide Production

    Sustainable manufacturing often feels like a buzzword, yet the impact becomes real at the shop floor level. Process chemistry for 3,3'-Dihydroxydiphenyl Disulfide has traditionally used aromatic solvents and oxidants with considerable waste burden. Several years back, we invested in solvent recovery units, which now reclaim nearly three-quarters of our organic waste stream, reducing both cost and environmental liability.

    Energy use also drew our attention. The disulfide-forming step runs under heating, so thermal energy recovery loops now channel waste heat to pre-warm feedstock streams. These efforts cut our fuel consumption and annual emissions measurably; our audited environmental reports show a 15% drop in greenhouse gas output over the last three years. While regulatory demands pushed us to update our systems, the reality is that material and energy efficiency supports a more stable business—the less waste we generate, the more consistent our pricing remains.

    As the global market trends toward cleaner, safer chemicals, we monitor emerging alternatives. While there are “greener” accelerators and antioxidants entering the field, the unique structure of 3,3'-Dihydroxydiphenyl Disulfide still delivers a mix of performance and cost that keeps it relevant. We engage directly with buyers to support recycling and safe disposal efforts—offering practical guidance, not empty claims. No chemical manufacturer stands alone on these issues, but we take direct, ongoing responsibility for minimizing our environmental footprint.

    Technical Support Rooted in Practical Experience

    Questions arise at every corner of a technical purchase: will this batch dissolve cleanly, will it introduce color bodies, will it behave the same way as the last shipment? Our technical support reflects lived experience, not scripted responses. From the plant operations desk to the customer service queue, staff field calls on everything from solubility in various plasticizers to potential sulfur mapping in XRF tests.

    We keep on hand a growing archive of customer formulations—strictly confidential, built up from years of problem-solving side by side. Some partners struggled with rapid setting in rubber sheets; others questioned why their mold release failed on certain runs; still others flagged minor odor concerns post-vulcanization. In each case, open communication between production chemists and client engineers led to troubleshooting grounded in reality. Sometimes, that means adjusting a feed rate, swapping packaging, or tweaking the particle size window. The goal: no batch leaves our plant without a clear picture of how it will perform at full scale.

    Collaboration does not end once the product is out the door. We provide follow-up, not as a formality but as a matter of pride. Supply interruptions, purity discrepancies, and application misfits receive prompt attention. If a client faces unique requirements—say, food-contact compliant production or ultra-low odor—our R&D team evaluates the feasibility, testing small pilot runs and providing honest feedback. We value the trust our partners place in us as the original manufacturer. Product reliability and solution-oriented support define that trust, more than a line on a sales invoice ever could.

    Challenges and Long-Term Outlook

    Every specialty chemical faces cycles of demand, cost pressure, and regulatory shifts. For 3,3'-Dihydroxydiphenyl Disulfide, the main hurdles tie directly to feedstock volatility and evolving end-use compliance standards. Supply chains for phenolic intermediates suffered spikes during regional slowdowns. In those moments, our in-house procurement and inventory teams dug in, qualifying alternate sources, building long-term partnerships, and keeping raw stock at levels high enough to blunt short-term shocks. While this may challenge just-in-time inventory philosophies, it has shielded us—and our downstream users—from the worst market disruptions.

    Regulation grows stricter. We track international standards and update our compliance documents to match both REACH and local requirements. Finished products using our disulfide can face extra scrutiny regarding migration, extractables, and hazardous decomposition products. We keep customers informed as new limits approach, and we work with them to supply COAs and full disclosure on known impurities and potential trace residues.

    The next stage may bring changes we are already preparing for: alternative accelerators based on aliphatic structures, biobased phenol options, or even non-aromatic curing chemistry. We have partnered with academic labs and commercial users to run early-stage comparative trials. Even in scenarios where 3,3'-Dihydroxydiphenyl Disulfide ultimately gives way to new innovations, we see a bright future for the insight, process discipline, and project management skills our staff have built. We take pride not in a single molecule, but in the ability to respond to new challenges with practical, science-driven adaptability.

    Dedicated to Reliability and Knowledge Sharing

    From research chemists to operations staff, everyone in our company cares about delivering material that meets the needs of today’s toughest compounders. 3,3'-Dihydroxydiphenyl Disulfide stands out not for a single benchmark, but for a track record backed by years of hands-on production, continuous testing, and responsive service. Feedback from frontline rubber technologists, process engineers, and plastics researchers drives our ongoing improvements—whether that means refining purity, sharpening particle size distribution, or supporting customer audits on demand.

    Industry trends shift rapidly. We believe adaptability, openness, and an unwavering attention to detail will keep both our product—and our knowledge—valuable for years to come. We welcome dialogue across the value chain. Every shipment reflects not just what we produce, but how we produce it. That is the real difference a manufacturer can offer.