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1-Propyl-3-Methylimidazolium Dicyanamide

    • Product Name 1-Propyl-3-Methylimidazolium Dicyanamide
    • Alias [PMIM][DCA]
    • Einecs 634-743-8
    • Mininmum Order 1 g
    • Factory Site Tengfei Creation Center,55 Jiangjun Avenue, Jiangning District,Nanjing
    • Price Inquiry admin@sinochem-nanjing.com
    • Manufacturer Sinochem Nanjing Corporation
    • CONTACT NOW
    VTB
    Specifications

    HS Code

    878370

    Chemical Name 1-Propyl-3-Methylimidazolium Dicyanamide
    Abbreviation [PMIM][DCA]
    Molecular Formula C9H14N6
    Molar Mass 206.25 g/mol
    Appearance colorless to pale yellow liquid
    Density 1.07 g/cm³ (at 25°C)
    Melting Point -34°C
    Boiling Point Decomposes before boiling
    Solubility In Water miscible
    Cas Number 514215-10-0

    As an accredited 1-Propyl-3-Methylimidazolium Dicyanamide factory, we enforce strict quality protocols—every batch undergoes rigorous testing to ensure consistent efficacy and safety standards.

    Packing & Storage
    Packing Amber glass bottle, 100g, with tight-seal cap, hazard labels, white chemical-resistant label: “1-Propyl-3-Methylimidazolium Dicyanamide, 100g, CAS# 64601-49-6.”
    Shipping 1-Propyl-3-Methylimidazolium Dicyanamide should be shipped in tightly sealed containers, away from moisture and incompatible materials. Package securely to prevent leaks or breakage. Use appropriate hazard labeling, and comply with all relevant regulations for shipping chemicals. Transport in a cool, well-ventilated environment. Handle with care to avoid exposure and environmental contamination.
    Storage 1-Propyl-3-Methylimidazolium Dicyanamide should be stored in a tightly sealed container, away from moisture, heat, and direct sunlight. Keep in a cool, dry, and well-ventilated area, separated from incompatible substances such as strong oxidizers and acids. Ensure proper labeling, and avoid exposure to air to prevent hydrolysis or degradation. Always follow local chemical storage regulations and safety guidelines.
    Application of 1-Propyl-3-Methylimidazolium Dicyanamide

    Applications of 1-Propyl-3-Methylimidazolium Dicyanamide in Industrial Manufacturing

    1-Propyl-3-Methylimidazolium Dicyanamide serves as a highly specialized ionic liquid, supporting advanced processes across fine chemical synthesis, electrochemical production, cellulose processing, and metal surface engineering. The following application sections reflect major industrial downstream uses based on our manufacturing practices and customer production requirements.

    1. Electrolyte Component in Supercapacitor Manufacture

    Large-scale supercapacitor producers increasingly rely on ionic liquid-based electrolytes to achieve higher voltage stability and extended operational temperature ranges. 1-Propyl-3-Methylimidazolium Dicyanamide offers excellent ionic conductivity and thermal tolerance, integrally supporting energy storage cell filling after electrode preparation. Its stable electrochemical window enhances device safety and service life, meeting the rigorous demands of next-generation electrical storage. Technical adoption is focused in mass production environments optimizing power density, cycling life, and reduced self-discharge. Careful quality control and batch traceability play a critical role in alignment with certified production frameworks.

    Industry compliance standards

    • IEC 62576: Secondary cells and batteries containing alkaline or other non-acid electrolytes
    • RoHS 2011/65/EU for restricted substance usage
    • ISO 9001:2015 for quality management in electronic components
    • UL 810A for electrolyte containment safety

    Typical usage ratio

    • Employed at 85–100 wt% as the major electrolyte fluid; minor additives (up to 15%) may refine conductivity or viscosity based on cell design and electrode material compatibility.

    Downstream process integration

    • Injected into cell casing during final assembly, directly after electrode sheets insertion and before terminal sealing.

    Final product types

    • High-energy density EDLC supercapacitor modules
    • Hybrid lithium-ion capacitors
    • Power system backup supercapacitors
    • Grid stabilization capacitor banks

    2. Solvent for Homogeneous Catalysis in Fine Chemical Synthesis

    This ionic liquid provides an advanced reaction medium for homogeneous transition metal-catalyzed syntheses of pharmaceuticals, agrochemicals, and specialty polymers. Its negligible vapor pressure promotes safer, more sustainable working conditions compared to traditional volatile organic solvents. In multi-step syntheses such as C–C bond formation, dicyanamide anion properties play an active role in stabilizing catalytic intermediates. Chemists adjust composition and solvent ratios according to target reaction rates, selectivity metrics, and downstream purification strategies. Batch and continuous flow settings both benefit from its thermal resilience and easy post-reaction separation.

    Industry compliance standards

    • ICH Q7A: GMP for Active Pharmaceutical Ingredients
    • REACH Regulation (EC) No 1907/2006 for chemical safety
    • ISO 14001 for environmental management of manufacturing facilities
    • U.S. EPA green chemistry practices

    Typical usage ratio

    • Applied as a primary reaction medium at 40–80 vol% of the total solvent system; specific loading depends on substrate solubility and catalyst requirements, adjusted during scale-up.

    Downstream process integration

    • Charged to the reactor at the initial solvent charging stage, prior to reactant and catalyst introduction, and remains present throughout reaction and separation steps.

    Final product types

    • Active pharmaceutical ingredients (APIs)
    • Agrochemicals (e.g. herbicide intermediates)
    • Polymer precursor monomers
    • High-value specialty chemicals

    3. Dissolution Aid for Cellulose Fiber and Film Processing

    Manufacturers of regenerated cellulose films and fibers utilize ionic liquids for dissolving wood pulp and other cellulosic feedstock under mild conditions. 1-Propyl-3-Methylimidazolium Dicyanamide ensures rapid cellulose solubilization, permitting direct spinning or casting processes without prior derivatization. The ionic environment leads to fibers with superior mechanical and adsorption properties, supporting applications in filtration, hygiene, and biocompatible textiles. Material selection and process tuning center on cost-effective recovery, impurity management, and byproduct minimization throughout batch manufacturing cycles.

    Industry compliance standards

    • ISO 1833: Textile fiber examination methods
    • Oeko-Tex Standard 100 for textile chemical safety
    • REACH Regulation (Annex XVII) for restricted substances in fibers
    • ISO 9001:2015 quality management in fiber production

    Typical usage ratio

    • Charged at 80–96 wt% of the solvent system for cellulose processing; the proportion is clarified based on cellulose concentration and desired final fiber properties.

    Downstream process integration

    • Blended with feedstock in the pre-spinning dissolver before extrusion through spinnerets or casting for film formation.

    Final product types

    • Regenerated cellulose fibers (Lyocell-type)
    • High-transparency cellulose films
    • Filtration membrane rolls
    • Medical-grade absorbent wovens

    4. Metal Plating and Surface Treatment Electrolyte Additive

    Advanced electronic and component plating lines incorporate ionic liquids to improve deposit uniformity and reduce surface defects. 1-Propyl-3-Methylimidazolium Dicyanamide, leveraged as an additive or carrier phase in nonaqueous electrolytes, enables precise control of deposition rates, grain structure, and adhesion properties for base metals and alloys. Use in pulse-plating regimes supports functional and decorative coatings with improved performance under demanding operational cycles. Our manufacturing partners emphasize process validation, waste minimization, and strict monitoring of impurity buildup in recirculating bath systems.

    Industry compliance standards

    • ISO 4527:2014 for electroplated coatings
    • IPC-4552 for electrodeposited copper on printed boards
    • ISO 14001 on environmental management in metal finishing
    • Restriction of Hazardous Substances (RoHS) compliance

    Typical usage ratio

    • Employed at 5–20 vol% in electroplating baths depending on desired deposit thickness and alloy system; ratios are refined based on plating current and target surface morphology.

    Downstream process integration

    • Added during initial electrolyte make-up and consistently monitored throughout automated or batch plating cycles on metal substrates.

    Final product types

    • Multilayer printed circuit board foils
    • Corrosion-resistant fastener coatings
    • Electronic contact surfaces
    • Tool and die plating finishes
    Free Quote

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    Certification & Compliance
    More Introduction

    1-Propyl-3-Methylimidazolium Dicyanamide: Setting New Standards through Hands-On Experience

    Understanding the Product through Real Manufacturing

    For the last decade, our team has worked with ionic liquids daily, watching trends shift and technology evolve all over the chemical industry. Among these, 1-Propyl-3-Methylimidazolium Dicyanamide stands out. Our process begins with attention to purity and stability above all else—customers depend on consistency to keep their labs and plants running. We’ve handled thousands of kilograms yearly, each batch meeting the same measurement for water content, halide levels, and physical characteristics. We’ve watched competitors focus on scale, but we focus on refinement and application. This difference shows through every drum and flask.

    From Production to Application: The Chemistry that Counts

    Our production technicians have learned the quirks of 1-Propyl-3-Methylimidazolium Dicyanamide by touching, testing, and tweaking countless procedures. Unlike many other imidazolium ionic liquids, this variant—bearing the dicyanamide anion—offers remarkable thermal stability and a much more manageable viscosity at room temperature. Chemists tell us how it refuses to crystallize easily, which streamlines dosing and transfer compared to those old, sticky salts others remember from grad school.

    Teams rely on this material in tasks beyond simple solvation. We’ve worked closely with research institutes and process engineers using it as a reaction medium for organometallic synthesis and various electrochemical applications, as well as serving as a supporting electrolyte in capacitors. A handful of high-throughput labs say they see substrate selectivity open up compared to chloride or hexafluorophosphate analogs, often simplifying downstream work-up. As true as that is, the hands-on difference shows up in the repeatability of results: cells operate longer, catalysts survive harsher cycles, and product isolation steps become less resource-intensive.

    Why the Dicyanamide Makes a Difference

    After years in production, we notice that customers who switched from tetrafluoroborate or bis(trifluoromethylsulfonyl)imide salts often report easier waste treatment and lower toxicity. Standard imidazolium liquids carrying halogenated anions frequently generate regulatory headaches. In contrast, our dicyanamide version cuts down on secondary halide emissions and lessens environmental risk in many operations. We sourced and qualified our raw materials to guarantee longevity and shelf stability without hidden degradation—something often overlooked outside the production line.

    Our warehouse crews have an easy time storing and transporting this material since it doesn’t clump during changes in humidity. We don’t hide behind big claims—this is just everyday experience. We pour from containers in both summer and winter without freeze-ups or blockages. Operators in outside locations appreciate that this material doesn’t require heating jackets or constant agitation, and these small savings have a way of scaling up across multiple shifts and production runs.

    Real-World Usage: What Sets Ours Apart

    Working as a manufacturer teaches you which claims matter and which fall flat. Early on, a major university tested three ionic liquids from us, all with similar cation structures. The 1-Propyl-3-Methylimidazolium Dicyanamide moved through their pipettes without the stickiness or gelling they experienced with other options. This isn’t about minor preferences; it solves workflow bottlenecks, improves throughput, and reduces cross-contamination on shared equipment.

    Colleagues in crystal engineering and separation science choose our product because it doesn't degrade nor does it darken when exposed to air for routine periods. Its low viscosity helps in keeping equipment clean—no clogged columns or pumps. This advantage turns into shorter downtime for cleaning and faster turnaround between syntheses. Our QC technicians take pride in monitoring every batch for color and clarity, catching trace contaminants before they cause trouble in customer workflows.

    Not All Ionic Liquids Are Built Equal

    We’ve fielded questions on why our 1-Propyl-3-Methylimidazolium Dicyanamide outperforms others. The real answer comes back to practical experience. Smaller particle size of the final material means less sediment at the bottom of containers, and careful drying yields a consistently low water content, under 0.1% by Karl Fischer titration. From the synthesis stage, we operate under a closed system, cutting down on potential exposure to atmospheric CO2 or moisture, both of which change the performance during precise chemical procedures.

    The lack of halides in this product translates into broader compatibility with transition-metal catalysts. Catalysts last longer before poisoning or precipitation, especially in cross-coupling and C-H activation chemistry. Companies in electroplating and organic synthesis have shifted entire workflows over to this formulation due to the low corrosivity and its unique solvation power with polar substrates.

    Model and Specifications: What Practical Experience Reveals

    Through the years, our team selected a model specification balancing purity and stability. In our experience, a purity greater than 99% (by HPLC/GC) is required by serious laboratories. Every lot gets checked for residual starting materials by NMR and for heavy metals using ICP-MS. Density sits around 1.05 g/cm3 at 20°C. The product remains a clear liquid at temperatures as cool as -10°C and holds steady up to about 160°C before thermal decomposition sets in. Viscosity and conductivity have tight specification windows, both critical to process chemists and engineers.

    All these attributes come from years solving headaches for customers. Research labs doing sensitive electrochemistry or those trialing new batteries regularly comment on the high reproducibility between shipments. Pharmaceutical companies use our ionic liquid for microwave-assisted synthesis, telling us that no residual unknown peaks appear in their product analytics, something that slows down scale-up with other suppliers.

    Real Production Challenges and Lessons Learned

    As the ones who monitor reactors and clean up spills, we’ve seen firsthand how impurities sneak in through poor process control. That’s why strict batch traceability and internal controls on drying and storage make an obvious difference. For the first few years, we wrestled with cation methyl impurities affecting viscosity. Only after hundreds of iterations did we pinpoint a solution, and our current process now catches each deviation long before filling drums.

    We’ve also mitigated operator error by introducing analytical checkpoints, confirming dicyanamide anion integrity by IR and mass spectrometry each time, and verifying that none of the raw materials degrade during transfer. Real-life applications revealed that users rarely want just the lab scale or the bulk quantity—they need both. So, we maintain both glass-packed ampoules for smaller scale R&D and antistatic-lined drums for those running pilot or production-level syntheses.

    Improvement Didn’t Stop with Scale-Up

    Growing from pilot to full-scale production meant making changes: installing dedicated stainless-steel lines, isolating dicyanamide feedstocks, and upgrading analytics with 21 CFR Part 11–compliant systems so customers could trust our data trail. This focus on operational transparency means clients in regulated industries receive information that matches their reporting and validation requirements. Nobody wants last-minute surprises on compliance audits, and our experience means the paperwork matches the chemical quality in practice.

    We train everyone at the plant to catch off-odors or discoloration before shipping, and rotating staff with deep product familiarity reduces the chance of mistakes. These improvements didn’t appear in manuals—they came from split drums, long nights restocking, and years of direct feedback from power users in the field.

    Environmental Impact and Safer Chemistry

    Our operations manager always says, “People want fewer headaches, not extra steps.” The lower hazard profile of dicyanamide-based ionic liquids has made this product a solid choice for companies facing tighter workplace safety and environmental rules. Classic imidazolium salts sometimes bring disposal difficulties or corrosion of plant hardware. With our formulation, users sidestep many of these legacy problems.

    We’ve partnered on joint pilot trials, substituting in this product where halide-rich ionic liquids dominated. Customers noticed not only fewer environmental compliance issues but reduced downtime linked to fouled pumps or leached equipment. It comes back to the manufacturing—taking time to filter and polish each batch avoids long-term buildup of trace metals or polymeric byproducts, which can accelerate equipment wear.

    Comparison to Competing Products

    From the plant floor, some differences become obvious with side-by-side work. Lower viscosity at operational temperatures allows quicker mixing and separation, giving faster cycle times across chemical synthesis and electrochemistry lines. As production staff, we handle live loading and dispensing, and we see first-hand that our product’s lack of “oiliness”—the slow pour, clingy residue seen in some older ionic liquids—means there’s much less material loss per batch.

    The real-world effect is clear. Several competitors’ ionic liquids introduce issues with phase separation, clouding, or microcrystalline precipitation after a few months on a shelf. Our own material remains optically clear even after a year under room temperature storage, so customers pull what they need without sifting for solids or cursing blocked dispensing tubes.

    Case Experience and Industry Insight

    Collaborating with academic centers, we’ve seen this product enable higher ionic conductivities in experimental supercapacitors due to its high ion mobility. Battery research teams push our 1-Propyl-3-Methylimidazolium Dicyanamide to upper voltage limits, reporting less oxidative decomposition than they expected. This matches literature but takes on more weight when it comes from seasoned researchers running constant cycles.

    In the industrial coatings segment, one of our long-term partners cut out fluorinated salts, replacing them with this ionic liquid to meet low-emission targets. Their production line measured a drop in hazardous waste output and reported fewer shut-downs for cleaning. In separations, customers observed sharper, more reproducible peaks in ion-exchange processes compared to methylimidazolium tetrafluoroborate, reflecting the influence of the dicyanamide anion’s coordination ability.

    Looking Ahead: Future Needs, Real Solutions

    We continue to listen closely to customers in specialist synthesis, battery research, and green chemistry disciplines. A growing number demand higher purity and ever-tighter specification windows. As a manufacturer, it’s on us to increase batch sizes without trading away these attributes: repeated testing at each scale-up step secures this.

    Instead of chasing every new market, we stick to what we know best—making sure the next batch matches the last, locking down the fundamental details that drive complex chemistry forward. From what we’ve seen, every breakthrough in ionic liquid applications starts with dependable, reproducible raw materials handled by people who understand their impact, from shop floor to research bench.

    Conclusion: Lessons from the Production Line

    Years of direct hands-on work with 1-Propyl-3-Methylimidazolium Dicyanamide has taught us the gap between promising specs on paper and reliable results in the reactor. Our customers’ feedback shapes daily production: whether it’s ease of handling, chemical stability, or reducing the hidden costs of cleaning and waste management, each aspect matters because we’ve managed all those steps ourselves.

    Our product’s track record comes not from marketing but from the reality of making and using it on both small and large scales. External certifications and audits confirm quality, but the difference lies in experience—every time someone pours, stirs, or samples from one of our drums, they use a material that reflects countless hours of troubleshooting, testing, and a continuous drive for improvement. This is what sets true manufacturing apart from trading or repacking, and why our 1-Propyl-3-Methylimidazolium Dicyanamide holds its reputation among chemists who demand accuracy and reliability in their work.