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1,3-Dichloro-2-Butene

    • Product Name 1,3-Dichloro-2-Butene
    • Alias 1,3-Dichloro-2-butylene
    • Einecs 211-221-8
    • Mininmum Order 1 g
    • Factory Site Tengfei Creation Center,55 Jiangjun Avenue, Jiangning District,Nanjing
    • Price Inquiry admin@sinochem-nanjing.com
    • Manufacturer Sinochem Nanjing Corporation
    • CONTACT NOW
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    Specifications

    HS Code

    881773

    CAS_Number 540-43-0
    Molecular_Formula C4H6Cl2
    Molecular_Weight 125.00 g/mol
    IUPAC_Name 1,3-dichlorobut-2-ene
    Appearance Colorless to light yellow liquid
    Density 1.167 g/cm3 at 20°C
    Melting_Point -85°C
    Boiling_Point 117-118°C
    Flash_Point 29°C (closed cup)
    Solubility_in_Water Insoluble
    Refractive_Index 1.468 at 20°C
    Vapor_Pressure 15 mmHg at 25°C

    As an accredited 1,3-Dichloro-2-Butene factory, we enforce strict quality protocols—every batch undergoes rigorous testing to ensure consistent efficacy and safety standards.

    Packing & Storage
    Packing A 500 mL amber glass bottle with a secure screw cap, labeled "1,3-Dichloro-2-Butene" and hazard warnings.
    Shipping 1,3-Dichloro-2-butene should be shipped in tightly sealed, corrosion-resistant containers, clearly labeled with hazard information. It must be transported according to local, national, and international regulations for toxic and environmentally hazardous substances, typically under UN number 2350. Keep away from heat, sparks, and incompatible materials. Use appropriate protective and safety measures during handling.
    Storage Store 1,3-Dichloro-2-butene in a cool, dry, well-ventilated area, away from sources of heat, ignition, and direct sunlight. Use tightly sealed, clearly labeled containers made of compatible materials. Keep away from strong oxidizers, acids, or bases. Ensure local exhaust ventilation and use appropriate chemical storage cabinets. Prevent container damage and follow all regulatory guidelines for hazardous chemical storage.
    Application of 1,3-Dichloro-2-Butene

    Applications of 1,3-Dichloro-2-Butene in Industrial Manufacturing

    As a direct manufacturer of 1,3-dichloro-2-butene, we support a focused range of advanced industrial sectors where this intermediate plays an integral role in synthesis and polymerization workflows. Below, we detail key downstream applications verified within the specialty chemical, polymer, and agrochemical industries, prioritizing regulatory compliance, technical formulation requirements, process integration points, and resulting product types.

    1. Synthesis of Fluorinated Agrochemical Intermediates

    Major agrochemical producers incorporate 1,3-dichloro-2-butene as a key chlorinated olefin intermediate for further fluorination during the synthesis of herbicides and insecticides. Use centers on halogen exchange reactions, where its efficient double bond reactivity enables precise functional group incorporation for advanced crop protection compounds.

    Industry compliance standards

    • Regulation (EC) No 1107/2009 for plant protection products (EU)
    • US EPA 40 CFR Part 180: Tolerances and Exemptions for Pesticide Chemical Residues
    • ISO 9001:2015 Certified Manufacturing Controls
    • REACH Registration, Evaluation, Authorization and Restriction of Chemicals (EU)

    Typical usage ratio

    • 5–18% w/w in halogen exchange feed per batch; varies by desired substituent and target molecule complexity

    Downstream process integration

    • Added during early-stage chlorination or fluorination in multi-step active ingredient synthesis
    • Often used in continuous-flow reactors for controlled conversion

    Final product types

    • Active ingredients for non-selective and selective herbicides
    • Precursors for pyrazole-based insecticides
    • Chlorinated or fluorinated crop protection intermediates

    2. Production of Ion-Exchange Resin Monomers

    Specialty polymer manufacturers use 1,3-dichloro-2-butene to introduce chloroalkene moieties in the synthesis of functionalized monomers for ion-exchange resins. The compound’s double-bond architecture enables tailored cross-linking, impacting resin porosity and selectivity profiles demanded by water treatment and chromatographic applications.

    Industry compliance standards

    • NSF/ANSI 61: Drinking Water System Components—Health Effects (US)
    • EU Regulation No 10/2011 for plastic materials intended for food contact
    • ISO 14001:2015 for environmental management systems in specialty resin plants
    • Good Manufacturing Practice (GMP) for polymer additives

    Typical usage ratio

    • 1–6% by weight of total monomer in batch or continuous suspension polymerization; selected for targeted resin exchange capacity

    Downstream process integration

    • Introduced at monomer blend stage prior to radical initiation
    • Often co-polymerized with styrenic or acrylate units for structural diversity

    Final product types

    • Cationic and anionic ion-exchange resin beads
    • Chromatography separation media
    • Deionization cartridges for water purification

    3. Synthesis of Intermediates for Pharmaceutical Chemicals

    Pharmaceutical synthesis sites require 1,3-dichloro-2-butene as a reagent to prepare halogenated building blocks. Its functionality supports the formation of ring systems and side chains in advanced intermediates used by API manufacturers, especially where site-specific substitution or alkylation is a critical design step.

    Industry compliance standards

    • ICH Q7A: Good Manufacturing Practice Guidelines for Active Pharmaceutical Ingredients
    • USP/NF standards for pharmaceutical intermediates
    • 21 CFR Part 211, FDA cGMP for finished pharmaceuticals
    • EudraLex Volume 4 for medicinal product manufacturing (EU)

    Typical usage ratio

    • 3–12% w/w per step, depending on target intermediate complexity and substitution demands

    Downstream process integration

    • Charged for nucleophilic halogenation, olefin addition, or ring closure reactions
    • Typically handled in closed-system R&D or pilot line reactors for impurity control

    Final product types

    • Pyrrole, pyrazole, and imidazole core intermediates
    • Halogenated specialty building blocks for API synthesis
    • Modified small molecules for proprietary drug discovery pipelines

    4. Modified Polymer Additive for Chlorinated Elastomer Manufacture

    Elastomer compounding plants apply 1,3-dichloro-2-butene in the synthesis of high-chlorine content copolymers to enhance thermal resistance and chemical stability. Its controlled addition allows precise molecular weight adjustment and cross-link density, critical for upgraded performance in seals, gaskets, and wire insulation.

    Industry compliance standards

    • ASTM D2000: Classification System for Rubber Products in Automotive Applications
    • UL 94: Flammability standards for polymeric materials
    • RoHS Directive 2011/65/EU for hazardous substances in electrical/electronic equipment
    • ISO 9001:2015 for manufacturing quality control

    Typical usage ratio

    • 2–10 phr (parts per hundred rubber) in compounding blends; adjusted for targeted chlorine incorporation based on evolving end-use specifications

    Downstream process integration

    • Blended with raw elastomer in open-mill or internal mixer before vulcanization
    • Can be metered in continuously during mastication or in batch post-polymerization functionalization

    Final product types

    • Automotive hose and seal compounds
    • Heat-resistant cable and wire sheathing
    • Chlorinated synthetic rubber gaskets and industrial belts
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    Certification & Compliance
    More Introduction

    1,3-Dichloro-2-Butene: Practical Chemical Solutions Direct from Our Facility

    A Manufacturer’s Take on 1,3-Dichloro-2-Butene

    Over the years, working on the production floor and in process control labs, we have learned that chemicals either pull their weight or they don’t. 1,3-Dichloro-2-Butene, which carries the CAS number 30116-09-1, does more than hold its own in industrial applications. Chemists and engineers who depend on robust intermediates see immediate value in this compound’s unique blend of reactivity and stability.

    We approach this material as makers who have fielded customer requests, re-engineered batch processes, and observed market trends up close. Questions about model numbers and grades come in regularly, but the heart of the discussion is always about what the chemical enables—and what problems it solves on the plant floor. Our standard production model features a minimum assay of 98%, with a clear, pale liquid appearance. For plants embedding this intermediate into more demanding syntheses, we have pushed the purification process further to supply materials with even stricter impurity specifications upon request.

    Hands-On Experience: Observations from Our Manufacturing Line

    A real appreciation for 1,3-Dichloro-2-Butene comes from seeing drums loaded and tankers pulled. Early on, a major customer in the agrochemical business asked for a reliable flow of this intermediate for a key coupling reaction. Their process depended on the Z-isomer for selectivity, but supply chain hiccups with inconsistent isomer ratios from various sources led to batch failures. In such situations, a manufacturer’s knowledge base makes all the difference. We tuned the isomeric purity specifically for their needs, and the plant’s yield swings flattened out.

    Companies making flame retardants and specialty polymers often send in samples for side-by-side trials, comparing performance between 1,3-Dichloro-2-Butene and other vinyl chloride-based starting materials. The real gain comes not just from the purity or concentration, but the internal control over trace water and residual chlorinated by-products. During high-temperature synthesis, small compositional differences have outsized effects. Handling these details at the manufacturing stage, not as an afterthought, supports more predictable results for downstream users.

    Comparing Theory and Field Work: Where 1,3-Dichloro-2-Butene Shines

    Testing shows that 1,3-Dichloro-2-Butene stands apart from mono-chlorinated or brominated analogs, as well as from other dichlorobutenes. Unlike 3,4-dichlorobutene or the isomeric 2,3-dichloro-1-butene, the molecule’s particular structure puts both chlorine atoms on the terminal and internal carbon atoms. Synthesis routes involving this configuration take advantage of differential reactivity, mapping closely to what chemists want when building up larger, more complex molecules.

    During manufacturing scale-up, we’ve run comparative trials to see which intermediates handle, store, and blend best with common reactants in pharmaceutical and pesticide processes. 1,3-Dichloro-2-Butene often comes out ahead: the boiling point around 120-122°C fits a variety of standard distillation and purification setups, and the reactivity works well for both nucleophilic substitution and addition reactions.

    Why Chemical Structure Matters in Daily Operations

    Years ago, we faced a growing demand from clients involved in specialty organic synthesis—a market that prizes not just the name but the behavior under pressure. In one project, a pharmaceutical firm hit a bottleneck using 1,4-dichloro-2-butene, struggling to reach clean yields during halogen exchange steps. Their review of published literature hinted at better success with our material. A switch brought more consistent results, reduced waste in their downstream steps, and ultimately cut costs.

    Real-world feedback reveals the gap between what looks fine on a spec sheet and what creates complications in the reactor or final product. Impurities like residual stabilizers, hydrolysis products, or heavy ends can creep in anywhere. Continuing investment in automation and batch analytics at our plant means tighter compositional control and cleaner outcomes, which in turn helps users focus on their core reactions rather than troubleshooting raw material inconsistencies.

    Main Uses as Seen by Producers

    We see three core industries consistently seeking out 1,3-Dichloro-2-Butene: agrochemicals, flame retardants, and specialty chemicals. Many agricultural chemical innovators select this intermediate for its ability to introduce vicinal dichloro groups with selective reactivity—a feature not shared by mono-chlorinated counterparts. The compound enters various steps for synthesizing fungicides, insecticides, and growth regulators.

    Polymer and material companies, on the other hand, often look for vinyl-based compounds with higher chlorine content for building flame retardant resins. 1,3-Dichloro-2-Butene serves as an efficient branching point for copolymerization or addition reactions. Its balance of volatility and functional group accessibility helps streamline production without complex workarounds.

    Several fine chemical producers have worked with us to substitute other dichlorinated butenes or four-carbon analogs with this compound, not for marketing reasons, but because 1,3-Dichloro-2-Butene brings cleaner performance profiles. Switching saves steps and reduces side product burden.

    Comparing with Other Chemicals: The Outcome in Practice

    We have carried out side-by-side reactivity tests with 1,2-dichlorobutene, 1,4-dichlorobutene, and a range of mono-chlorobutenes in collaboration with users. The stepwise addition or exchange of chlorine atoms is more straightforward with our product, enabling cleaner linking to aromatic rings or further chlorination as needed. Performance gains become obvious in scale-up runs.

    Customers report that compared to 1,4-dichloro-2-butene, the chlorine placement in 1,3-dichloro-2-butene offers different selectivity during key steps. This reduces purification load and raises yield. Compared to mono-chlorinated analogs, which tend to give more mixture and less clean final product, the dichloro version streamlines synthesis, especially in multi-step campaigns.

    Practical Know-How: Handling and Storage

    Handling practices make a noticeable difference. While standard chemical compatibility checks cover the basics, our operators have developed routines to minimize exposure to moisture, which can impact storage time. Tanks and drums stored in ventilated, dry environments show longer shelf life without caking or phase separation. We use stainless steel or lined containers, depending on project scope.

    Our team tracks every lot for specification drift—not only at shipment but during storage at customer sites. We encourage direct feedback from end users. Slight color changes or viscosity shifts signal either temperature variation or early-stage hydrolysis, so we work with partners to recommend simple, effective storage solutions. These details, overlooked by traders or third-party brokers, become obvious only when you’re the one fielding service calls after business hours.

    Specification: Not Just Numbers, But Process Confidence

    While datasheets list purity thresholds and standardized impurity tables, practical knowledge shapes how a lot performs in real synthesis. We replicate customer process variables—including reaction time, pressure swings, and catalyst exposures—during pilot batch tests. Details like trace water, acid numbers, or chlorine distribution hold real meaning in larger runs. By listening to consistent issues—residual odor, color shifting, or compatibility with base solvents—we’ve continued to refine purification steps and container linings.

    Our published model sits at 98% minimum assay and a low moisture content. Inline GC checks watch for common side products, helping to keep output within a tighter range than minimum standards require. This attention to process tracking comes from years of troubleshooting with plants taking our material through to API, crop protection, or high-performance resin production.

    Supporting Process Improvement and Accountability

    Many process chemists look for certainty—a steady, predictable behavior across dozens of plant runs and scale-ups. Our open-door development approach means sharing failure data as well as success stories. In the early days, one batch drifted upward in a specific impurity due to a seemingly minor tweak in the cooling cycle. The affected lots got quarantined and replaced, but more importantly, the correction went into the process flow, stopping recurrence. Users downstream could keep their campaigns on schedule without sudden surprises.

    Third-party testers and auditors sometimes call for explanations about trace organics or out-of-spec samples. Because we own the reaction, we document the actual material balance, side stream management, and line cleaning between different production runs. Technicians logging readings on site catch drift before it becomes a shipment problem, feeding transparency and trust into the system.

    Looking Beyond: Regulatory and Practical Questions

    Chemicals like 1,3-Dichloro-2-Butene come under scrutiny at multiple levels. End users navigate evolving local and international regulations, and we understand the need for continuous communication. Over the years, we have worked alongside clients to prepare for audits in Europe, North America, and Asia. Most questions focus on trace contaminants, storage conditions, or reactivity under transport conditions.

    Knowing how the material performs in actual process conditions, not just what’s on paper, supports regulatory compliance and safe implementation. When larger-scale users investigate switching suppliers or scaling up, we arrange technical briefings to share historical data, lessons learned, and practical operating limits. Our approach favors reliability and constant improvement—qualities that show in smoother approvals and fewer regulatory headaches for everyone involved.

    Current Trends and Tackling Future Challenges

    Market demand fluctuates based on agricultural cycles, resin innovations, and regulatory shifts. Rather than chasing these trends reactively, we aim to anticipate them through research collaborations and regular user engagement. For example, recent years have seen growth in demand from specialty polymer developers shifting from brominated to chlorinated intermediates. Early discussions with their scientists gave us the time to test and validate what 1,3-Dichloro-2-Butene could offer for high-performance plastics, before their procurement teams even finalized orders.

    Key challenges ahead include supply chain resilience and environmental responsibility. As a full-process manufacturer, we invest heavily in solvent recovery and emission control, aiming to reduce waste and energy use without raising costs. These investments reflect both a commitment to sustainable production and the everyday realities of running a large chemical operation in a changing world.

    Lessons Learned: Chemical Production as Craft and Science

    Manufacturing 1,3-Dichloro-2-Butene has been shaped as much by direct customer conversation as by classic organic chemistry. Surprises occur—a small leak, a lot out of spec, a novel application request. By staying close to the process and the people who rely on it, innovation emerges from daily hands-on work as well as larger R&D projects.

    Each application, from plant protection to specialty resins, comes with specific hurdles. Designing a process for clean, reproducible batches means understanding not just theoretical chemistry, but the gritty realities of operations. We carry out plant tours for technical teams, organize post-shipment check-ins, and field phone calls about process hiccups. These exchanges constantly inform adjustments to reactor conditions, purification steps, and logistics.

    Direct Support: Manufacturer’s Role in Industry Progress

    Our facility has grown up alongside changes in automation, supply chain digitization, and market globalization. What remains constant is the need for clear, timely technical support. Our production and QC staff remain available to troubleshoot, share best practices for handling and integration, and gather outcome data from user sites.

    Many users look for more than just a monthly batch or a tonnage guarantee—they want a manufacturing partner who can provide hand-on knowledge about process control, blending, and troubleshooting. By delivering direct support, we help customers avoid costly rework and material waste. Over the long run, steady collaboration replaces uncertainty with concrete improvements.

    Summary of Practical Advantages

    1,3-Dichloro-2-Butene stands out for its direct applicability and reliability in high-volume chemical processes. Over years of continuous production and applied technical problem solving, this chemical has cemented its place among key intermediates used in modern industry. Its strengths—a combination of structural adaptability, predictable performance, and ease of integration—set it apart from competitors.

    From our perspective as a producer involved in hundreds of unique projects, the biggest difference between this and similar chemicals remains its steady behavior in varied conditions and the close relationship we build with industrial users adjusting recipes or scaling up operations. Consistent quality, direct communication, and deep process knowledge allow everyone in the chain—from operators to R&D teams—to achieve better results with less risk.

    Working with Us

    Producing and supplying 1,3-Dichloro-2-Butene is not just about meeting a spec. It means working with partners who understand manufacturing realities and who take joint responsibility for process outcomes. As innovation continues in agrochemicals, advanced resins, and specialty synthesis, producer and customer alike increasingly rely on a foundation of reliability, transparency, and shared technical learning.

    From onsite audits to remote troubleshooting, our teams remain committed to turning lessons learned into better products and more resilient processes. By handling both the chemistry and the practical realities, we support users in reaching new levels of efficiency, consistency, and performance in their own plants.